Digitization entails the conversion of traditional library materials such as printed books and papers into digital formats where they can be stored and manipulated by a computer. This paper discussed digitization of library resources, process, and challenges at the Federal University of Technology, Owerri. The article outlined the advantages of digitization and further revealed some hurdles that prevent effective digitization in Nigerian academic libraries with particular reference to FUTO library. These challenges include among others: inadequate funding, erratic power supply, lack of modern infrastructure, lack of skilled staff and nonchalant attitude of departments. Also, the paper explored efforts made so far by the management of FUTO library in addressing the challenges of digitization.